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33421-40-8 2-Amino-5-phenylpyridine

33421-40-8 2-Amino-5-phenylpyridine

2-AMINO-5-PHENYLPYRIDINE Basic information 2-AMINO-5-PHENYLPYRIDINE Chemical Properties Safety Information MSDS Information 2-AMINO-5-PHENYLPYRIDINE Usage And Synthesis 2-AMINO-5-PHENYLPYRIDINE Preparation Products And Raw materials Upstream information 5-phenylpyridin-2-amine; bromobenzene;...

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Product Details:

2-AMINO-5-PHENYLPYRIDINE Basic information

Product Name:

2-AMINO-5-PHENYLPYRIDINE

Synonyms:

2-amino-5-phenyl-pyridin; 5-PHENYL-2-PYRIDINAMINE; 5-PHENYL-PYRIDIN-2-YLAMINE; AKOS BAR-1613; 2-AMINO-5-PHENYLPYRIDINE; PHE-P-1; 2-pyridinaMine, 5-phenyl-; 2-Amino-5-phenylpyridine, 97%

CAS:

33421-40-8

MF:

C11H10N2

MW:

170.21

EINECS:


Product Categories:

pharmacetical; Aromatics Compounds; Aromatics; Amines; Heterocycles

Mol File:

33421-40-8.mol

image001.png

 

2-AMINO-5-PHENYLPYRIDINE Chemical Properties 

Appearance:

Beige Crystalline Solid

Density:

1.133g/cm3

Melting Point:

132ºC

Boiling Point:

323.6ºC at 760mmHg

Flash Point:

175.6ºC

Refractive Index:

1.625

storage temp. 

-20°C Freezer

CAS DataBase Reference

33421-40-8(CAS DataBase Reference)

 

Safety Information 

Hazard Codes 

Xn

Risk Statements 

36/37/38-36-22-40

Safety Statements 

26-36/37/39-36/37

RTECS 

US2145000

 

MSDS Information 


2-AMINO-5-PHENYLPYRIDINE Usage And Synthesis 


Chemical Properties

Beige Crystalline Solid

Uses

A product from the pyrolysis of phenylalanine

Intermediate as

1427782-89-5 IWP-L6

image003_副本.jpg

Synthesis route

image005_副本.jpg

Reference:

Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie European Journal of Organic Chemistry, 2012 , # 3 p. 595 – 603

 

image007_副本.jpg

Reference:

1. Qiao, Lixin; Choi, Sungwoon; Case, April; Gainer, Thomas G.; Seyb, Kathleen; Glicksman, Marcie A.; Lo, Donald C.; Stein, Ross L.; Cuny, Gregory D. Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 21 p. 6122 - 6126

2. Russian Journal of General Chemistry, , vol. 66, # 12 p. 1925 - 1938

3. Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie European Journal of Organic Chemistry, 2012 , # 3 p. 595 – 603

4. European Journal of Organic Chemistry, # 3 p. 595 - 603

 

image009_副本.jpg

Reference:

Stoll, Ion; Mix, Andreas; Rozhenko, Alexander B.; Neumann, Beate; Stammler, Hans-Georg; Mattay, Jochen Tetrahedron, 2008 , vol. 64, # 17 p. 3813 – 3825

 

image011_副本.jpg

Reference:

Bunzen, Jens; Hovorka, Rainer; Luetzen, Arne Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5228 – 5236

 

image013_副本.jpg

Reference:

Knize, Mark G.; Felton, James S. Heterocycles, 1986 , vol. 24, # 7 p. 1815 – 1819

 

image015_副本.jpg

Reference:

Bristol-Myers Company Patent: US4122274 A1, 1978 ; US 4122274 A

 

2-AMINO-5-PHENYLPYRIDINE Preparation Products And Raw materials

 

Upstream information

5-phenylpyridin-2-amine; bromobenzene; phenylboronic acid; 5-iodopyridin-2-amine; 2-Amino-5-chloropyridine; oleic acid; 4, 4, 5, 5-tetramethyl-2-phenyl-1,3, 2-dioxaborolane; 2-Chloro-5-phenylpyridine; 3-Phenylpyridine; 5-(4, 4, 5, 5-Tetramethyl-1, 3, 2-dioxaborolan-2-yl)pyridin-2-amine;


Downtream information

2-Iodo-5-phenylpyridine; 2-Bromo-5-phenylpyridine; 3-N-methyl-5-phenylpyridine-2, 3-diamine; 2-Amino-3-bromo-5-phenylpyridine; 5-phenylpyridin-2-amine; 3-Phenylpyridin-2-ylamine; PhIP; biphenyl;


2-AMINO-5-PHENYLPYRIDINE Basic information

Product Name:

2-AMINO-5-PHENYLPYRIDINE

Synonyms:

2-amino-5-phenyl-pyridin; 5-PHENYL-2-PYRIDINAMINE; 5-PHENYL-PYRIDIN-2-YLAMINE; AKOS BAR-1613; 2-AMINO-5-PHENYLPYRIDINE; PHE-P-1; 2-pyridinaMine, 5-phenyl-; 2-Amino-5-phenylpyridine, 97%

CAS:

33421-40-8

MF:

C11H10N2

MW:

170.21

EINECS:


Product Categories:

pharmacetical; Aromatics Compounds; Aromatics; Amines; Heterocycles

Mol File:

33421-40-8.mol

image001.png


2-AMINO-5-PHENYLPYRIDINE Chemical Properties

Appearance:

Beige Crystalline Solid

Density:

1.133g/cm3

Melting Point:

132ºC

Boiling Point:

323.6ºC at 760mmHg

Flash Point:

175.6ºC

Refractive Index:

1.625

storage temp.

-20°C Freezer

CAS DataBase Reference

33421-40-8(CAS DataBase Reference)


Safety Information

Hazard Codes

Xn

Risk Statements

36/37/38-36-22-40

Safety Statements

26-36/37/39-36/37

RTECS

US2145000


MSDS Information


2-AMINO-5-PHENYLPYRIDINE Usage And Synthesis


Chemical Properties

Beige Crystalline Solid

Uses

A product from the pyrolysis of phenylalanine

Intermediate as

1427782-89-5 IWP-L6

image003_副本.jpg

Synthesis route

image005_副本.jpg

Reference:

Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie European Journal of Organic Chemistry, 2012 , # 3 p. 595 – 603


image007_副本.jpg

Reference:

1. Qiao, Lixin; Choi, Sungwoon; Case, April; Gainer, Thomas G.; Seyb, Kathleen; Glicksman, Marcie A.; Lo, Donald C.; Stein, Ross L.; Cuny, Gregory D. Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 21 p. 6122 - 6126

2. Russian Journal of General Chemistry, , vol. 66, # 12 p. 1925 - 1938

3. Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie European Journal of Organic Chemistry, 2012 , # 3 p. 595 – 603

4. European Journal of Organic Chemistry, # 3 p. 595 - 603


image009_副本.jpg

Reference:

Stoll, Ion; Mix, Andreas; Rozhenko, Alexander B.; Neumann, Beate; Stammler, Hans-Georg; Mattay, Jochen Tetrahedron, 2008 , vol. 64, # 17 p. 3813 – 3825


image011_副本.jpg

Reference:

Bunzen, Jens; Hovorka, Rainer; Luetzen, Arne Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5228 – 5236


image013_副本.jpg

Reference:

Knize, Mark G.; Felton, James S. Heterocycles, 1986 , vol. 24, # 7 p. 1815 – 1819


image015_副本.jpg

Reference:

Bristol-Myers Company Patent: US4122274 A1, 1978 ; US 4122274 A


2-AMINO-5-PHENYLPYRIDINE Preparation Products And Raw materials


Upstream information

5-phenylpyridin-2-amine; bromobenzene; phenylboronic acid; 5-iodopyridin-2-amine; 2-Amino-5-chloropyridine; oleic acid; 4, 4, 5, 5-tetramethyl-2-phenyl-1,3, 2-dioxaborolane; 2-Chloro-5-phenylpyridine; 3-Phenylpyridine; 5-(4, 4, 5, 5-Tetramethyl-1, 3, 2-dioxaborolan-2-yl)pyridin-2-amine;


Downtream information

2-Iodo-5-phenylpyridine; 2-Bromo-5-phenylpyridine; 3-N-methyl-5-phenylpyridine-2, 3-diamine; 2-Amino-3-bromo-5-phenylpyridine; 5-phenylpyridin-2-amine; 3-Phenylpyridin-2-ylamine; PhIP; biphenyl;


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