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99769-19-4 3-Methoxycarbonylphenylboronic Acid

99769-19-4 3-Methoxycarbonylphenylboronic Acid

3-Methoxycarbonylphenylboronic acid Basic information 3-Methoxycarbonylphenylboronic acid Chemical Properties Safety Information 3-Methoxycarbonylphenylboronic acid Usage And Synthesis 3-Methoxycarbonylphenylboronic acid Preparation Products And Raw materials Upstream information...

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Product Details:

3-Methoxycarbonylphenylboronic acid Basic information

Product Name:

3-Methoxycarbonylphenylboronic acid

Synonyms:

METHYL 3-BORONOBENZOATE;3-METHOXYCARBONYLPHENYLBORONIC ACID;3-(METHOXYCARBONYL)BENZENEBORONIC ACID;AKOS BRN-0125;M-(METHOXYCARBONYL)PHENYLBORONIC ACID;3-METHOXYCARBONYLPHENYLBARONIC ACID;3-(Methoxycarbonyl)phenylboronic Acid (contains varying amounts of Anhydride);3-Methoxycarbonylphenylboronic acid,97%

CAS:

99769-19-4

MF:

C8H9BO4

MW:

179.97

EINECS:


Product Categories:

blocks;BoronicAcids;Carboxes;Acids and Derivatives;Boron, Nitrile, Thio,&   TM-Cpds;Boronic acids;Aryl;Ester;Organoborons;B (Classes of Boron Compounds);Boronic acid;CHIRAL CHEMICALS;Aromatics;Boron Derivatives;Intermediates & Fine Chemicals;Pharmaceuticals;Boronate Ester;Potassium Trifluoroborate

Mol File:

99769-19-4.mol

image001.gif


3-Methoxycarbonylphenylboronic acid Chemical Properties

form

Powder

color

White to off-white

Appearance:

White to light yellow crystal powder

Density:

1.25g/cm3

Melting Point:

187-191ºC

Boiling Point:

359.9ºC at 760 mmHg

Flash Point:

171.5ºC

Refractive Index:

1.532

Storage Condition:

Refrigerator (+4ºC)

Water Solubility

Reacts with water.

CAS DataBase Reference

99769-19-4(CAS DataBase Reference)


Safety Information

Hazard Codes

Xi

Risk Statements

36/37/38

Safety Statements

37/39-26-36

WGK Germany

3

Hazard Note

Irritant

HazardClass

IRRITANT

Hs code

2931900090


3-Methoxycarbonylphenylboronic acid Usage And Synthesis

Chemical Properties

White to light yellow crystal powde

Uses

Used in the preparation of substituted pyrazolylpyrimidinamine derivative for use as protein kinase inhibitors.

Uses

suzuki reaction

Intermediate as


Synthesis route

image003_副本.jpg

Reference:

Wang, Xiao-Jun; Sun, Xiufeng; Zhang, Li; Xu, Yibo; Krishnamurthy, Dhileepkumar; Senanayake, Chris H. Organic Letters, 2006 , vol. 8, # 2 p. 305 - 307


image005_副本.jpg

Reference:

Journal of the American Chemical Society, vol. 134, # 28 p. 11667 - 11673


image007_副本.jpg

Reference:

Organic Letters, vol. 14, # 18 p. 4814 - 4817,4


3-Methoxycarbonylphenylboronic acid Preparation Products And Raw materials

Raw materials

Tetrahydrofuran-->Magnesium-->Triisopropyl   borate-->Bis(2-dimethylaminoethyl)   ether-->Methyl   3-iodobenzoate


Upstream information

4-Bromobenzaldehyde; 3-Iodobenzoic acid; 2-bromopyridine; 2,3-dimethylbutane-2,3-diol; methanol; 1-Iodo-4-nitrobenzene; 3-Methoxycarbonylphenylboronic acid; Methyl 3-bromobenzoate; 4-Bromo-2-nitrophenol; zinc,dicyanide;


Downtream information

methyl 3-azidobenzoate; Methyl 4'-nitro-[1,1'-biphenyl]-3-carboxylate; 3-(4-hydroxy-3-nitrophenyl)benzoic acid; methyl 3-(3-methoxycarbonylphenyl)benzoate; Methyl 3-(trifluoromethyl)benzoate; Methyl 3-Fluorobenzoate; methyl 3-(4-formylphenyl)benzoate; Methyl 3-Cyanobenzoate; 3-Methoxycarbonylphenylboronic acid; 5-(3-methoxycarbonylphenyl)furan-2-carboxylic acid


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