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5332-25-2 6-Bromoquinoline

5332-25-2 6-Bromoquinoline

6-Bromoquinoline Chemical Properties Safety Information 6-Bromoquinoline Usage And Synthesis 6-Bromoquinoline Preparation Products And Raw materials Upstream information 4,6,8-tribromoquinoline; Downtream information 6,8-Dibromoquinoline; 4,6-DIBROMOQUINOLINE

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Product Details:

6-Bromoquinoline Basic information

Bromoquinoline Application and synthetic method


Product Name:

6-Bromoquinoline

Synonyms:

6-Bromo-1-azanaphthalene;6-Bromoquinoline,97%;6-Br-quinoline;6-BROMOQUINOLINE;TIMTEC-BB SBB001559;6-bromo-quinolin;Quinoline, 6-bromo-;6-BROMOQUINOLINE 95+%

CAS:

5332-25-2

MF:

C9H6BrN

MW:

208.05

EINECS:

206-363-3

Product Categories:

blocks;Bromides;Quinolines;Halides;Quinolines, Isoquinolines & Quinoxalines;Quinoline&Isoquinoline;Miscellaneous;Quinoline Derivertives;Aromatics Compounds;Haloquinolines;quinoline;Aromatics;Heterocycles;Quinolines, Isoquinolines & Quinoxalines;Boronic Acid;Heterocyclic Compounds;Building Blocks;Halogenated Heterocycles;Heterocyclic Building Blocks;QuinolinesHeterocyclic Building Blocks

Mol File:

5332-25-2.mol

image001_副本.jpg


6-Bromoquinoline Chemical Properties

Appearance:

Light Yellow Colour Liquid

Density:

1.564 g/cm3

Melting Point:

19ºC

Boiling Point:

278ºC at 760 mmHg

Flash Point:

132.8ºC

Refractive Index:

n20/D 1.663

Storage Condition:

Refrigerator

solubility

Soluble in acetone, acetonitrile, dichloromethane, ethyl acetate and THF.

CAS DataBase Reference

5332-25-2(CAS DataBase Reference)

NIST Chemistry Reference

6-Bromo quinoline(5332-25-2)

EPA Substance Registry System

Quinoline, 6-bromo-(5332-25-2)


Safety Information

Hazard Codes

Xi,Xn

Risk Statements

36/37/38-41-37/38-22-20/21/22

Safety Statements

26-37/39-39-36

Hazard Note

Irritant

TSCA

Yes

HazardClass

IRRITANT

Hs code

2933499090


6-Bromoquinoline Usage And Synthesis

Bromoquinoline

There are seven positional isomers   of bromoquinoline and their main properties are listed below:w::

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Application and synthetic method

3-bromo-quinoline is reacted with mixed acid for generating 3-bromo-5-nitro-quinoline, which heats together with potassium permanganate for being oxidation into 5-bromo-2, 3-pyridine dicarboxylic acid.
6-bromo-quinoline is heated together with nitric acid to generate 6-bromo-8-nitro quinolone with further reaction with potassium permanganate for being oxidized to 2, 3-pyridinedicarboxylic acid.
2-bromo-quinolien can be synthesized through the reaction between 2-hydroxy quinoline and phosphorus pentabromide.
Quinoline perbromide is heated at 180 °C for generating 3-bromo-quinoline.
From the heating between 4-hydroxy quinoline and phosphorus pentabromide, or from the diazotization reaction via 4-aminoquinoline to generate 4-bromo-quinoline;
5-bromo-quinoline is synthesize by the heating reaction between m-bromo-aniline, glycerol, m-bromo nitrobenzene and concentrated sulfuric acid, or from the diazotization reaction of 5-aminoquinoline.
6-bromo-quinoline can be synthesized from the heating of bromoaniline, glycerol, concentrated sulfuric acid, and p-bromo-nitrobenzene. 7-bromo-quinoline can be synthesized from the diazotization reaction of 7-aminoquinoline.
8-bromo-quinoline can be synthesized from the heating reaction of o-bromo-aniline, glycerol, concentrated sulfuric acid and o-bromo nitrobenzene.
application: as organic synthesis reagents.

Chemical Properties

Thick Oil

Intermediate as

1022150-57-7 SGX-523, 943540-75-8   JNJ-38877605


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6-Bromoquinoline Preparation Products And Raw materials

Raw materials

Sodium   hydroxide-->Sulfuric   acid -->Tetrahydrofuran-->Toluene-->1-Butanol-->Zinc   chloride-->Glycerol-->Acrolein-->4-Bromoaniline-->Chloranil-->1-Bromo-4-nitrobenzene


Upstream information

4,6,8-tribromoquinoline;


Downtream information

6,8-Dibromoquinoline; 4,6-DIBROMOQUINOLINE


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