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10365-98-7 3-Methoxyphenylboronic Acid

3-Methoxyphenylboronic acid Basic information 3 - Methoxyphenylboronic acid Preparation Products And Raw materials 3-Methoxyphenylboronic acid Usage And Synthesis Upstream information Ethyl Carbonocyanidate ; tris(2-methylpropyl)borate ; benzocaine ; phenylboronic acid ; 4-Chlorophenylboronic acid;...

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Product Details:

3-Methoxyphenylboronic acid Basic information

Product Name:

3-Methoxyphenylboronic    acid

Synonyms:

M-METHOXYPHENYLBORONIC ACID; BORONIC ACID, (3-METHOXYPHENYL)-; AKOS BRN-0015; 3-METHOXYBENZENEBORONIC ACID; 3-METHOXYPENYLBORONIC ACID; 3-METHOXYPHENYLBORONIC ACID; M-METHOXYPHENYLBORIC ACID

CAS:

10365-98-7

MF:

C7H9BO3

MW:

151.96

EINECS:

1312995-182-4

Product Categories:

blocks; Boronic Acids; Boronic Acid series; Boron , Nitrile, Thio,& TM-Cpds;Substituted Boronic Acids; Boronic acids; Boronic    Acid; Aryl;Organoborons;B    (Classes of Boron Compounds); Boronic Acids & Esters; Phenyls & Phenyl-Het; Aromatics; Boron Derivatives; Boronate    Ester; Potassium    Trifluoroborate

Properties

Appearance & Physical State:

white to light  yellow crystal powder

Density:

1.17 g/cm3

Melting Point:

160-163ºC

Boiling Point:

318.6ºC at 760 mmHg

Flash Point:

146.5ºC

Refractive Index:

1.524

Storage Condition:

0-6ºC

Vapor Pressure:

0.000149mmHg at  25°C

Safety Info

Symbol:

image002_副本.jpg      GHS07

Sign:

Warning

hazard declaration:

H302; H315; H319; H335

hazard declaration add:

 

waring notice:

P261; P305 + P351 + P338

Safety Statements:

S26-S37/39

HS Code:

2931900090

WGK Germany:

3

Risk Statements:

R36/37/38

Hazard Codes:

Xi


3-Methoxyphenylboronic acid Preparation Products And Raw materials

Raw materials

Tetrahydrofuran-->n-Butyllithium-->Triisopropyl    borate-->3-Bromoanisole


3-Methoxyphenylboronic acid Usage And Synthesis

Uses

3-Methoxylphenylboronic Acid is a phenylboronic acid used to investigate boron function in plants.

Uses

suzuki reaction

Intermediate as

546141-08-6 URB597, 1431985-92-0 K02288 and 395104-30-0 CC401 and 887264-45-1 JP104

image004_副本.jpg


       

image006_副本.jpg


       

image008_副本.jpg

       

image010_副本.jpg

Synthesis route

image012_副本.jpg

Reference:

Tetrahedron, , vol. 69, # 19 p. 3934 - 3941
US2002/198251 A1
Journal of Medicinal    Chemistry, , vol. 47, # 23 p. 5612 - 5615

image014_副本.jpg

Reference:

Tetrahedron Letters, , vol. 45, # 35 p. 6657    - 6660


Upstream information

Ethyl Carbonocyanidate ; tris(2-methylpropyl)borate; benzocaine; phenylboronic acid; 4-Chlorophenylboronic acid; chlorobenzene; 2-iodophenol; 4-Bromochlorobenzene ; 4'-Bromoacetophenone; 1-Bromo-2-nitrobenzene;


Downtream information

(3-methoxyphenyl)-(4-methoxyphenyl)methanone ; (3-methoxyphenyl)-(4-methylphenyl)methanone ; ethyl 2-(3-methoxyphenyl)-2-oxoacetate; 1-fluoro-3-(3-methoxyphenyl)benzene ; Pyridine hydrochloride ; 4-Methoxyphenylboronic acid ; 3'-Methoxybiphenyl-4-carboxylic acid; 3-nitroanisole ; 3-[2-(5-ethyl-3,4-diphenylpyrazol-1-yl)phenyl]phenol ; biphenyl

 

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