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182163-96-8 3,4,5-Trimethoxyphenylboronic Acid

182163-96-8 3,4,5-Trimethoxyphenylboronic Acid

3,4,5-Trimethoxyphenylboronic acid Basic information 3,4,5-Trimethoxyphenylboronic acid Chemical Properties Safety Information 3,4,5-Trimethoxyphenylboronic acid Usage And Synthesis 3,4,5-Trimethoxyphenylboronic acid Preparation Products And Raw materials Upstream information...

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Product Details:

3,4,5-Trimethoxyphenylboronic acid Basic information

Product Name:

3,4,5-Trimethoxyphenylboronic    acid

Synonyms:

RARECHEM AH PB 0050;AKOS BRN-0140;3,4,5-TRIMETHOXYBENZENEBORONIC ACID;3,4,5-TRIMETHOXYPHENYLBORONIC ACID;3,4,5-Trimethoxylphenylboronic acid;3,4,5-TRIMETHOXYBENZENEBORONIC ACID, 98+%;3,4,5-Trifluoromethoxyphenylboronic acid;3,4,5-Trimethoxyphenylboronic acid ,98%

CAS:

182163-96-8

MF:

C9H13BO5

MW:

212.01

EINECS:

 

Product Categories:

Substituted    Boronic Acids;Alkoxy;Aryl;Organoborons;Boronic acid;Boronic acid series;Boronic Acids;Boronic Acids and Derivatives;Boronic Acids

Mol File:

182163-96-8.mol

image001.gif


3,4,5-Trimethoxyphenylboronic acid Chemical Properties

Appearance:

beige crystalline powder

Density:

1.21 g/cm3

Melting   Point:

244-247ºC

Boiling   Point:

370.6ºC at 760mmHg

Flash    Point:

177.9ºC

Refractiv Index:

1.513

Storage Condition:

Refrigerator (+4ºC)

Vapor  Pressure:

3.79E-06mmHg at 25°C

BRN 

8205051

CAS DataBase Reference

182163-96-8(CAS    DataBase Reference)


Safety Information

Hazard Codes 

Xn,Xi

Risk Statements 

36/37/38-22-20/21/22

Safety Statements 

37/39-26-36

WGK Germany 

3

Hazard Note 

Irritant

Hs code

2931900090


3,4,5-Trimethoxyphenylboronic acid Usage And Synthesis

Chemical Properties

Beige crystalline powder

Uses

suzuki reaction

Intermediate as

1627503-67-6 LDN-214117 and    1431985-92-0 K02288
     

image003_副本.jpg

image005_副本.jpg

Synthesis route

image007_副本.jpg

Reference:

Rosen, Brad M.; Wilson, Daniela A.; Wilson,    Christopher J.; Peterca, Mihai; Won, Betty C.; Huang, Chenghong; Lipski,    Linda R.; Zeng, Xiangbing; Ungar, Goran; Heiney, Paul A.; Percec, Virgil Journal of the American Chemical Society, 2009 , vol. 131, # 47 p. 17500 -    17521
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz,    Hans-Guenther; Podesta, Julio C. European Journal of Organic Chemistry, 2009    , # 23 p. 3964 - 3972

image009_副本.jpg

Reference:

European Journal of Organic Chemistry, , # 15    p. 2829 - 2839

image011_副本.jpg

Reference:

Tetrahedron Letters, , vol. 44, # 24 p. 4443    - 4446
Fukuda, Tsutomu; Sudo,    Ei-ichi; Shimokawa, Kozue; Iwao, Masatomo Tetrahedron, 2008 , vol. 64, # 2 p.    328 - 338


3,4,5-Trimethoxyphenylboronic acid Preparation Products And Raw materials


Upstream information

(4-Nitrophenyl)boronic acid; Ethyl 2-Chloroisonicotinate; 3,4,5-Trimethoxyaniline; 5-chloro-2-phenyl-3,4-dihydropyrazole; 5-bromofuran-2-carbaldehyde;Ethyl 2-bromobenzoate; Allyl bromide; tert-butyl 2,5-dibromopyrrole-1-carboxylate; 5-bromo-1,2,3-trimethoxybenzene; 2,4-bis(3,5-di-tert-butyl-4-methoxyphenyl)-6-(3,4,5-trimethoxyphenyl)-1,3,5,2,4,6-trioxatriborinane;


Downtream information

2-phenyl-5-(3,4,5-trimethoxyphenyl)-3,4-dihydropyrazole; ethyl 2-(3,4,5-trimethoxyphenyl)pyridine-4-carboxylate; 4-anilinobutanenitrile; 3,5-Dimethylphenylboronic acid; 2,4-bis(3,5-dimethylphenyl)-6-(3,4,5-trimethoxyphenyl)-1,3,5,2,4,6-trioxatriborinane; (3,4,5-trimethoxyphenyl)boronic acid;Combretastatin A4; 2-(3,5-di-tert-butyl-4-methoxyphenyl)boronic acid; 3-bromo-7-(3,4,5-trimethoxyphenyl)thieno[3,2-c]pyridin-4-amine


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